About this dataset

The glass compositions of major elements have been analyzed at INGV-OE with Zeiss LEO-1430 scanning electron microscope, equipped with an INCA ENERGY Oxford Instruments EDS micro-analytical system (SEM-EDS). Analytical conditions are 20 keV of acceleration tension, 1200 nA of beam current and XPP data reduction routine. In order to minimize alkalis loss during analysis, a square raster of 10 microns is used. The accuracy of our measurements has been checked through replicate analyses of the international standard VG-2 Glass basaltic, USNM 111240/52 (Jarosewich et al., 1980). The precision, expressed as relative standard deviation, is less than 1% for SiO2, Al2O3, FeO, MgO and CaO and less than 3% for TiO2, MnO, Na2O, K2O and P2O5 (Miraglia, 2012).
The analyses have been performed in groundmass glass containing less than 15% microlites. Each measure is the average of 10 to 15 analyses.

Citation

  • Miraglia L. (2021). Etna Glass analyses 2013 (GMCET_2013) (Version 1) [Data set]. Istituto Nazionale di Geofisica e Vulcanologia (INGV). https://doi.org/10.13127/etna/gmc_2013
  • Miraglia L. (2012). Caratteristiche del sistema analitico SEM-EDS: valutazione dell'accuratezza e della precisione delle analisi eseguite su standards internazionali di minerali e vetri. Rapporti Tecnici INGV, n. 233. ISSN 2039-7941

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Technical description

Dataset Legend
Sample label: name identificative of the sample the Acronyms used for Etna summit craters are: VOR= Voragine Crater, BN=Bocca Nuova Crater, NEC=North-East Crater, SEC=South-East Crater, NSEC=New South-East Crate;
Sample Type: field characteristics of a sample (bomb,lapilli or ash);
Data emission: Date of sample eruption;
Activity type: description of the volcanic activity provided from the Access archive of the INGV-OE Petroteca.